Alright Janet — let's do this.
5. Mwang[i] set up an apparatus for finding the percentage of humus contents in a soil by ignition.
b) Outline the steps followed in carrying out the illustrated experiment.
Step 1: Outline the experimental procedure.
• Weigh a clean, dry crucible (M1).
• Add a known mass of oven-dried soil sample to the crucible. Weigh the crucible with the soil (M2).
• Place the crucible with the soil on a tripod stand with a gauze mat and heat it strongly using a Bunsen burner for a prolonged period, stirring occasionally.
• Allow the crucible and the remaining soil (ash) to cool completely in a desiccator.
• Weigh the crucible with the ash (M3).
• Repeat the heating, cooling, and weighing steps until a constant mass is obtained.
c) Explain what happens after heating the soil and its contents.
Step 2: Explain the changes during heating.
• Upon strong heating, the organic matter (humus) present in the soil undergoes combustion.
• This process converts the solid organic compounds into gaseous products such as carbon dioxide (CO2) and water vapor (H2O), which escape into the atmosphere.
• The remaining material in the crucible is primarily the inorganic mineral components of the soil, often appearing as a greyish-white ash.
d) Compare the mass after and before heating.
Step 3: Compare the masses.
• The mass of the soil after heating will be less than its mass before heating.
• This reduction in mass is attributed to the loss of organic matter that was burnt off and released as gases during the ignition process.
• The difference in mass (M2−M3) represents the mass of the organic matter (humus) originally present in the soil sample.
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